HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → HCID 178516908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | N-(4-chlorophenyl)benzene-1,2-diamine | HCID 522323 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178516908 | HCID 178516908 | — |
Reaction Steps
N-(4-Chlorophenyl)benzene-1,2-diamine (11.2 g) was added to diethyl oxalate (50 ml) and the mixture heated under reflux for 2 hours. The mixture was cooled and ethanol (40 ml) was added. The precipitated solid was filtered off and recrystallised from ethanol giving the title compound (11.2 g) mp>300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04296114 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-5f67bd962ece4c348acec0776cac1378 |
| Source note | uspto-grants-1981_10 |