HCID 70577148, compound → HCID 70577147, compound

HRID 848482Notes

Reaction equation

HRID 848482 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:17]3[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=3)[N:11]=[C:10]([NH:18][CH2:19][CH2:20][N:21]([CH2:24][CH3:25])[CH2:22][CH3:23])[C:9]2=[O:26])=[CH:4][CH:3]=1>C(Cl)(Cl)Cl>[ClH:1].[ClH:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:17]3[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=3)[N:11]=[C:10]([NH:18][CH2:19][CH2:20][N:21]([CH2:24][CH3:25])[CH2:22][CH3:23])[C:9]2=[O:26])=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 70577148HCID 70577148, compound

Product 1

HCID 70577147HCID 70577147, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

1-(4-Chlorophenyl)-1,2-dihydro-3-(N,N-diethylamino)ethylaminoquinoxalin-2-one (5.0 g) was dissolved in chloroform (150 ml) and dry hydrogen chloride was bubbled through the solution for 10 minutes. The precipitate was dried and recrystallised from ethanol giving the title compound mp >240° C.

Workup

  1. customdry hydrogen chloride was bubbled through the solution for 10 minutes
  2. customThe precipitate was dried
  3. customrecrystallised from ethanol giving the title compound mp >240° C.

Sources & evidence

ORD record
ord-a21151614f2b40ed92f2eff4c8947795
Source dataset
uspto-grants-1981_10
Patent number
US04296114

Reaction notes

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