N,N-Diethylethylenediamine → HCID 20565437, compound

HRID 848483Notes

Reaction equation

HRID 848483 reaction equation
Cl[C:2]1[C:7](=[O:8])[N:6]([C:9]2[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][CH:10]=2)[C:5]2[N:16]=[CH:17][CH:18]=[CH:19][C:4]=2[N:3]=1.[CH2:20]([N:22]([CH2:26][CH3:27])[CH2:23][CH2:24][NH2:25])[CH3:21]>C(O)C>[Cl:15][C:12]1[CH:13]=[CH:14][C:9]([N:6]2[C:7](=[O:8])[C:2]([NH:25][CH2:24][CH2:23][N:22]([CH2:26][CH3:27])[CH2:20][CH3:21])=[N:3][C:4]3[CH:19]=[CH:18][CH:17]=[N:16][C:5]2=3)=[CH:10][CH:11]=1

Participants

4

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 20565448HCID 20565448, compound

Product 1

HCID 20565437HCID 20565437, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Preparation as in Example 39 but using 2-chloro-4-(4-chlorophenyl)-3,4-dihydro-3-oxopyrido[2,3-b]pyrazine and N,N-diethylethylene diamine in refluxing ethanol gave the title compound mp 149°-150° C.

Workup

  1. customPreparation as in Example 39

Sources & evidence

ORD record
ord-b9b1f434fbb54eabb41f2fd92c8e3381
Source dataset
uspto-grants-1981_10
Patent number
US04296114

Reaction notes

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