N,N-Diethylethylenediamine → HCID 20565469, compound

HRID 848484Notes

Reaction equation

HRID 848484 reaction equation
Cl[C:2]1[C:7](=[O:8])[N:6]([C:9]2[CH:14]=[CH:13][C:12]([CH3:15])=[CH:11][CH:10]=2)[C:5]2[N:16]=[CH:17][CH:18]=[CH:19][C:4]=2[N:3]=1.[CH2:20]([N:22]([CH2:26][CH3:27])[CH2:23][CH2:24][NH2:25])[CH3:21]>C(O)C>[CH2:20]([N:22]([CH2:23][CH2:24][NH:25][C:2]1[C:7](=[O:8])[N:6]([C:9]2[CH:14]=[CH:13][C:12]([CH3:15])=[CH:11][CH:10]=2)[C:5]2[N:16]=[CH:17][CH:18]=[CH:19][C:4]=2[N:3]=1)[CH2:26][CH3:27])[CH3:21]

Participants

4

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 20565460HCID 20565460, compound

Product 1

HCID 20565469HCID 20565469, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Preparation as in Example 39 but using 2-chloro-3,4-dihydro-4-(4-methylphenyl)-3-oxopyrido[2,3-b]pyrazine and N,N-diethylethylene diamine in refluxing ethanol gave the title compound mp 131°-132° C.

Workup

  1. customPreparation as in Example 39

Sources & evidence

ORD record
ord-d612c74b48af44bfa30e089c19313ad9
Source dataset
uspto-grants-1981_10
Patent number
US04296114

Reaction notes

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