N,N-Diethylethylenediamine → HCID 20565488, compound

HRID 848485Notes

Reaction equation

HRID 848485 reaction equation
Cl[C:2]1[C:7](=[O:8])[N:6]([C:9]2[CH:14]=[CH:13][C:12]([O:15][CH3:16])=[CH:11][CH:10]=2)[C:5]2[N:17]=[CH:18][CH:19]=[CH:20][C:4]=2[N:3]=1.[CH2:21]([N:23]([CH2:27][CH3:28])[CH2:24][CH2:25][NH2:26])[CH3:22]>>[CH2:21]([N:23]([CH2:24][CH2:25][NH:26][C:2]1[C:7](=[O:8])[N:6]([C:9]2[CH:14]=[CH:13][C:12]([O:15][CH3:16])=[CH:11][CH:10]=2)[C:5]2[N:17]=[CH:18][CH:19]=[CH:20][C:4]=2[N:3]=1)[CH2:27][CH3:28])[CH3:22]

Participants

3

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 20565438HCID 20565438, compound

Product 1

HCID 20565488HCID 20565488, compound

Procedure

Preparation as in Example 39 but using 2-chloro-3,4-dihydro-4-(4-methoxyphenyl)-3-oxopyrido[2,3-b]pyrazine and N,N-diethylethylene diamine gave the title compound mp 167°-168° C.

Workup

  1. customPreparation as in Example 39

Sources & evidence

ORD record
ord-c7b9f8948b9a4613a39c9acc6da49649
Source dataset
uspto-grants-1981_10
Patent number
US04296114

Reaction notes

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