HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20565443, compound → HCID 20565468, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20565443 | HCID 20565443 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20565468 | HCID 20565468 | — |
Reaction Steps
A solution of 1-(4-chlorophenyl)-1,2,3,4-tetrahydroquinoxalin-2-one (8.2 g) in dichloromethane (50 ml) was stirred with manganese dioxide (10.0 g) for 4 hours. The mixture was filtered, evaporated, and the residue was recrystallised from ethanol giving the title compound mp 169°-171° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04296114 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-b812400383414fb39423b3d7606178bf |
| Source note | uspto-grants-1981_10 |