HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53411291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Propenoic acid, 3-(3-nitrophenyl)- | HCID 68390 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53411291 | HCID 53411291 | 91% |
Reaction Steps
A mixture of 50 g. of 3-(3-nitrophenyl)propenoic acid, 24.54 ml. of thionyl chloride and 300 ml. of benzene were heated under reflux for 2.5 hours. The cooled solution was filtered and then it was evaporated in vacuo. The residue was recrystallized from carbon tetrachloride, to give 49.9 g. (91% yield) of the title compound, m.p. 81°-83.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04296120 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-4bc709618a3446d399e48fd5ecd351b6 |
| Source note | uspto-grants-1981_10 |