Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Nitrobenzaldehyde → Ethyl 2-methyl-3-(4-nitrophenyl)prop-2-enoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Nitrobenzaldehyde | HCID 541 | — |
| 반응물 | Ethyl 2-(triphenylphosphoranylidene)propionate | HCID 79792 | — |
| 생성물 | Ethyl 2-methyl-3-(4-nitrophenyl)prop-2-enoate | HCID 54080096 | 56% |
반응 단계
The title compound was prepared from triphenyl(1-[ethoxycarbonyl]ethylidene)phosphorane and 4-nitrobenzaldehyde, substantially according to Preparation 5. The product was obtained in 56% yield, as an orange-yellow solid, m.p. 70.5°-73° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04296129 |
| 출처 데이터셋 | uspto-grants-1981_10 |
| ORD ID | ord-a0663b9c42bd49229061bb1cfe73b09c |
| 출처 메모 | uspto-grants-1981_10 |