Hydrochloric Acid → HCID 22359589, compound

Participants

Reaction Steps

3.55 g (0.01 mol) trichlorophloroglucinol triisopropylether in 100 ml isopropanol were mixed with 5 g sodium. Heating with reflux was continued until all sodium had been dissolved. This was followed by diluting with 100 ml water, neutralizing with hydrochloric acid of 15% by weight, taking up of the organic phase in ethyl ether, drawing off of the ethyl ether and distilling of the residue on a bulb tube (2-3 mbar, airbath temperature 130° to 150° C.). 2.47 g phloroglucinol triisopropylether were obtained, which corresponds to a yield of 98% of theoretical.

Provenance & Evidence