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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 848622Generated: October 29, 2026

Water → HCID 86738059, compound

https://huagongshe.com/reaction/848622

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantAluminium lithium hydrideHCID 21226445—
ReactantHCID 86738060HCID 86738060—
SolventDiethyl EtherHCID 3283—
ProductHCID 86738059HCID 8673805978%

Reaction Steps

To a solution of ethyl trans, trans, trans-2,4,7-undecatrienoate (4.7 g) in dry ether (200 ml) was added with stirring lithium aluminum hydride (1 g) under ice-cooling little by little. The mixture was stirred for an hour at the same temperature. To the resultant mixture was added ether containing water to give insoluble materials, which were removed by filtration. The organic layer was washed with water, dried over magnesium sulfate and concentrated under reduced pressure to give colorless oily trans, trans, trans-2,4,7-undecatrien-1-ol (3.4 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04297096
Source datasetuspto-grants-1981_10
ORD IDord-e990883f9f944e07bef2c9125d8d1b2c
Source noteuspto-grants-1981_10