HCID 86738059, compound → HCID 86738062, compound

Participants

Reaction Steps

To a solution of trans, trans, trans-2,4,7-undecatrien-1-ol (3.4 g) in chloroform (300 ml) was added manganese dioxide (30 g). The reaction mixture was stirred for 60 hours at ambient temperature. After the manganese dioxide was removed by filtration, the resultant mixture was concentrated under reduced pressure to give a yellowish oily residue, which was subjected to a column chromatography on silica gel (developing solvent: chloroform) to give colorless oily trans, trans, trans-2,4,7-undecatrienal (2 g).

Provenance & Evidence