HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → 2-Ethylhexanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | 1,2,6-Trimethyl-4(1H)-pyridinone | HCID 292248 | — |
| Product | 2-Ethylhexanoyl chloride | HCID 79103 | 89% |
Reaction Steps
This time, 10 mmols of N-methyl-2,6-dimethyl-4-pyridone were used and 117 g of phosgene were introduced in the course of 2 and a half hours. A yield of 89% of 2-ethylhexanoyl chloride was obtained, after distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04297301 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-209d2b095a704f55823227365638158b |
| Source note | uspto-grants-1981_10 |