HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene → n-Dodecylethyldichlorosilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene | HCID 6325 | — |
| Reactant | n-Dodecyldichlorosilane | HCID 123720552 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | n-Dodecylethyldichlorosilane | HCID 20564956 | — |
Reaction Steps
Resultant n-dodecyldichlorosilane in an amount of 161.4 g (0.6 mol), 22.4 g of ethylene (0.8 mol) and a solution of H2PtCl6 ·6H2O in isopropanol (0.05 mol % relative to n-dodecyldichlorosilane) were charged in a pressure-proof stainless steel reactor. After sealing, reaction was carried out at 50° C. for 25 hours to give n-dodecylethyldichlorosilane [(n--C12H25)(C2H5)SiCl2 ].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04297499 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-3fda26a631f947ffb97d341e6f053fd4 |
| Source note | uspto-grants-1981_10 |