HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octadecene → Octadecyldichlorosilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octadecene | HCID 8217 | — |
| Reactant | Dichlorosilane | HCID 61330 | — |
| Product | Octadecyldichlorosilane | HCID 102243275 | — |
Reaction Steps
Dichlorosilane in an amount of 60.6 g (0.6 mol), 176.4 g of 1-octadecene (0.7 mol) and 0.07 mol % of RhCl(PPh)3 (relative to dichlorosilane) were charged in a 500 ml pressure-proof stainless steel reactor. After sealing, reaction was carried out at 130° C. for 30 hours. The reacted liquid was distilled in vacuo to give n-octadecyldichlorosilane (n--C18H37SiHCl2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04297499 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-752d3d99fdca4c918514c3964109bad8 |
| Source note | uspto-grants-1981_10 |