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HRID 848827作成日:2026年10月25日

1-Hexene → Silane, dichlorodihexyl-

https://huagongshe.com/reaction/848827

反応式

関与物質

役割名称HCID仕込み量
反応物1-HexeneHCID 11597—
反応物DichlorosilaneHCID 61330—
触媒Chloroplatinic acidHCID 61859—
生成物Silane, dichlorodihexyl-HCID 87510—
生成物Dichloro(hexyl)silaneHCID 92038703—

反応手順

Dichlorosilane in an amount of 83.5 g (0.827 mol), 88.6 g of 1-hexene (1.08 mol) and 0.05 mol % of chloroplatinic acid (relative to dichlorosilane) were charged in a stainless steel reactor and sealed and subjected to reaction in a bath at a temperature of 50° C. for 5 hours. After reaction, the seal of the reactor was broken and the reacted liquid was discharged, and by vacuum distillation, n-hexyldichlorosilane was obtained with a yield of 18% and di-n-hexyldichlorosilane with a yield of 72%.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04297499
出典データセットuspto-grants-1981_10
ORD IDord-60d939a4befd475d8458e8f2b1973f22
出典メモuspto-grants-1981_10