HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 54560967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) | HCID 2735153 | — |
| Reactant | HCID 54084144 | HCID 54084144 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54560967 | HCID 54560967 | 99% |
Reaction Steps
The title material of Example 32 (0.50 g, 2.2 mmol) in CH2Cl2 (15 mL) and in the presence of 3A molecular sieves (1.0 g) was reacted with trimethyloxonium tetrafluoroborate (0.39 g, 2.6 mmol) by the method of Example 3 to produce 0.53 g (99%) of the title material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011028 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-8f5e4843415d481098c2b8e8c9926d1f |
| Source note | uspto-grants-2000_01 |