HCID 53952906, compound → HCID 18800796, compound

HRID 849065Notes

Reaction equation

HRID 849065 reaction equation
[C:1]1([CH:7]=[CH:8][CH2:9][CH:10]2[NH:17][C:16](=[O:18])[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>CO.[Pd]>[C:1]1([CH2:7][CH2:8][CH2:9][CH:10]2[NH:17][C:16](=[O:18])[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 1

HCID 53952906HCID 53952906, compound

Product 1

HCID 18800796HCID 18800796, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

The title material of Example 68 in MeOH is hydrogenated over Pd on carbon in a standard Parr apparatus by the method of Example 35 to generate the title product.

Sources & evidence

ORD record
ord-347aa60bb02c4f39a2e5f3077d8a9af1
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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