Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18800814, compound

HRID 849066Notes

Reaction equation

HRID 849066 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH:10]2[NH:17][C:16](=[O:18])[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.F[B-](F)(F)F.[CH3:24][O+](C)C>C(Cl)Cl>[CH3:24][O:18][C:16]1[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH:10]([CH2:9][CH2:8][CH2:7][C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[N:17]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 18800796HCID 18800796, compound

Product 1

HCID 18800814HCID 18800814, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 71 is reacted with trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-e8a48503efe94f1bbf424be9d672e76f
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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