Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 53861558, compound

HRID 849070Notes

Reaction equation

HRID 849070 reaction equation
[O:1]=[C:2]1[NH:8][CH:7]([CH:9]=[CH:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[CH2:6][CH2:5][CH2:4][CH2:3]1.F[B-](F)(F)F.[CH3:26][O+](C)C>C(Cl)Cl>[CH3:26][O:1][C:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH:7]([CH:9]=[CH:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[N:8]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 53662904HCID 53662904, compound

Product 1

HCID 53861558HCID 53861558, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 79 is reacted with trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-ed3fd3e66b9e4f44bc8aaf8359707c2a
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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