HCID 53662904, compound → HCID 18800827, compound

HRID 849072Notes

Reaction equation

HRID 849072 reaction equation
[O:1]=[C:2]1[NH:8][CH:7]([CH:9]=[CH:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[CH2:6][CH2:5][CH2:4][CH2:3]1>CO.[Pd]>[O:1]=[C:2]1[NH:8][CH:7]([CH2:9][CH2:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

4

Reactant 1

HCID 53662904HCID 53662904, compound

Product 1

HCID 18800827HCID 18800827, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

The title material of Example 79 in MeOH is hydrogenated over Pd on carbon in a standard Parr apparatus by the method of Example 35 to generate the title product.

Sources & evidence

ORD record
ord-1ef7efce23a94e28bc1ed4b4c2d1fd74
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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