Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18800830, compound

HRID 849073Notes

Reaction equation

HRID 849073 reaction equation
[O:1]=[C:2]1[NH:8][CH:7]([CH2:9][CH2:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[CH2:6][CH2:5][CH2:4][CH2:3]1.F[B-](F)(F)F.[CH3:26][O+](C)C>C(Cl)Cl>[CH3:26][O:1][C:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH:7]([CH2:9][CH2:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[N:8]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 18800827HCID 18800827, compound

Product 1

HCID 18800830HCID 18800830, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 82 is reacted with trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-767a27b06fb449679c9c6cacaad74db6
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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