HCID 54240556, compound → HCID 18800762, compound

HRID 849077Notes

Reaction equation

HRID 849077 reaction equation
[O:1]=[C:2]1[CH:8]([CH:9]=[CH:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[CH2:7][CH2:6][CH2:5][CH2:4][NH:3]1>CO.[Pd]>[O:1]=[C:2]1[CH:8]([CH2:9][CH2:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[CH2:7][CH2:6][CH2:5][CH2:4][NH:3]1

Participants

4

Reactant 1

HCID 54240556HCID 54240556, compound

Product 1

HCID 18800762HCID 18800762, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

The title material of Example 85 in MeOH is hydrogenated over Pd on carbon in a standard Parr apparatus by the method of Example 35 to generate the title product.

Sources & evidence

ORD record
ord-413f252965c14b489e0a9d69f27d7670
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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