Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18800869, compound

HRID 849078Notes

Reaction equation

HRID 849078 reaction equation
[O:1]=[C:2]1[CH:8]([CH2:9][CH2:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[CH2:7][CH2:6][CH2:5][CH2:4][NH:3]1.F[B-](F)(F)F.[CH3:26][O+](C)C>C(Cl)Cl>[CH3:26][O:1][C:2]1[CH:8]([CH2:9][CH2:10][C:11]2[CH:20]=[CH:19][CH:18]=[CH:17][C:12]=2[C:13]([O:15][CH3:16])=[O:14])[CH2:7][CH2:6][CH2:5][CH2:4][N:3]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 18800762HCID 18800762, compound

Product 1

HCID 18800869HCID 18800869, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 88 is reacted with trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-b6a21150d12a455abc50c0cd6baf7c4a
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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