HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Methyl 1-[2-(1,3-dioxan-2-yl)ethyl]-2-oxocyclohexanecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Cyclohexanecarboxylic acid, 2-oxo-, methyl ester | HCID 170489 | — |
| Reactant | 1,3-Dioxane, 2-(2-bromoethyl)- | HCID 520656 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Methyl 1-[2-(1,3-dioxan-2-yl)ethyl]-2-oxocyclohexanecarboxylate | HCID 18800662 | — |
Reaction Steps
A solution of 2-carbomethoxycyclohexanone in DMF is reacted with 2-(2-bromoethyl)-1,3-dioxane and potassium carbonate by the method of Example 102 to generate the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011028 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-89bcc112ee1949f392bc459e3e029417 |
| Source note | uspto-grants-2000_01 |