Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18800828, compound
Reaction equation
[C:1]1([N:7]2[C:11]([CH2:12][CH:13]3[NH:19][C:18](=[O:20])[CH2:17][CH2:16][CH2:15][CH2:14]3)=[CH:10][C:9]([C:21]([F:24])([F:23])[F:22])=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.F[B-](F)(F)F.[CH3:30][O+](C)C>>[CH3:30][O:20][C:18]1[CH2:17][CH2:16][CH2:15][CH2:14][CH:13]([CH2:12][C:11]2[N:7]([C:1]3[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=3)[N:8]=[C:9]([C:21]([F:23])([F:22])[F:24])[CH:10]=2)[N:19]=1Participants
3
Procedure
The title material of Example 137 is reacted with trimethyloxonium tetrafluoroborate by the method of Example 3 to generate the title compound.
Sources & evidence
- ORD record
- ord-b9a89f73504b4062b49097850b4a04a0
- Source dataset
- uspto-grants-2000_01
- Patent number
- US06011028
Reaction notes
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