Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18800849, compound

HRID 849107Notes

Reaction equation

HRID 849107 reaction equation
[C:1]1([N:7]2[C:11]([CH2:12][CH:13]3[NH:19][C:18](=[O:20])[CH2:17][CH2:16][CH2:15][CH2:14]3)=[CH:10][C:9]([C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.F[B-](F)(F)F.[CH3:32][O+](C)C>>[C:1]1([N:7]2[C:11]([CH2:12][CH:13]3[CH2:14][CH2:15][CH2:16][CH2:17][C:18]([O:20][CH3:32])=[N:19]3)=[CH:10][C:9]([C:21]3[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=3)=[N:8]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 18800791HCID 18800791, compound

Product 1

HCID 18800849HCID 18800849, compound

Procedure

The title product of Example 146 is reacted with trimethyloxonium tetrafluoroborate by the method of Example 3 to generate the title compound.

Sources & evidence

ORD record
ord-fb2f9cee0cfc41dba36f2ae25bbf214f
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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