Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 54360238, compound

HRID 849115Notes

Reaction equation

HRID 849115 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH:10]=[CH:11][CH:12]1[NH:18][C:17](=[O:19])[CH2:16][CH2:15][CH2:14][CH2:13]1)([O-:3])=[O:2].F[B-](F)(F)F.[CH3:25][O+](C)C>C(Cl)Cl>[CH3:25][O:19][C:17]1[CH2:16][CH2:15][CH2:14][CH2:13][CH:12]([CH:11]=[CH:10][C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N+:1]([O-:3])=[O:2])[N:18]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 54487678HCID 54487678, compound

Product 1

HCID 54360238HCID 54360238, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 155 is reacted with trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-d937c53c57d94d16831fb07eb2ebbf37
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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