HCID 178479062, compound → HCID 178478660, compound

HRID 849117Notes

Reaction equation

HRID 849117 reaction equation
[ClH:1].[N+:2]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[CH:11]=[CH:12][CH:13]1[NH:19][C:18](=[NH:20])[CH2:17][CH2:16][CH2:15][CH2:14]1)([O-])=O>CO.[Pd]>[ClH:1].[ClH:1].[NH:20]=[C:18]1[NH:19][CH:13]([CH2:12][CH2:11][C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[NH2:2])[CH2:14][CH2:15][CH2:16][CH2:17]1

Participants

4

Reactant 1

HCID 178479062HCID 178479062, compound

Product 1

HCID 178478660HCID 178478660, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

The title material of Example 157 in MeOH is hydrogenated over Pd on carbon in a standard Parr apparatus by the method of Example 35 reducing both the nitro and double bond functions to generate the title product.

Sources & evidence

ORD record
ord-ddbc6c3e51724d95a67b45105d348d56
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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