Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 54132952, compound

HRID 849118Notes

Reaction equation

HRID 849118 reaction equation
[O:1]=[C:2]1[NH:8][CH:7]([CH2:9][CH:10]=[CH:11][C:12]2[CH:21]=[CH:20][C:19]([N+:22]([O-:24])=[O:23])=[CH:18][C:13]=2[C:14]([O:16][CH3:17])=[O:15])[CH2:6][CH2:5][CH2:4][CH2:3]1.F[B-](F)(F)F.[CH3:30][O+](C)C>C(Cl)Cl>[N+:22]([C:19]1[CH:20]=[CH:21][C:12]([CH:11]=[CH:10][CH2:9][CH:7]2[CH2:6][CH2:5][CH2:4][CH2:3][C:2]([O:1][CH3:30])=[N:8]2)=[C:13]([CH:18]=1)[C:14]([O:16][CH3:17])=[O:15])([O-:24])=[O:23]

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 53791502HCID 53791502, compound

Product 1

HCID 54132952HCID 54132952, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 159 is reacted with trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-c81cb58f93d14a6a9734abfdd1963834
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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