HCID 53946614, compound → HCID 18800648, compound

HRID 849123Notes

Reaction equation

HRID 849123 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]2[NH:17][C:16](=[O:18])[CH2:15][CH2:14][CH2:13][CH2:12]2)[CH:6]=[CH:7][CH:8]=1>CO.[Pd]>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:9][CH2:10][CH:11]2[NH:17][C:16](=[O:18])[CH2:15][CH2:14][CH2:13][CH2:12]2)[CH:6]=[CH:7][CH:8]=1

Participants

4

Reactant 1

HCID 53946614HCID 53946614, compound

Product 1

HCID 18800648HCID 18800648, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

The title material of Example 163 in MeOH is hydrogenated over Pd on carbon in a standard Parr apparatus by the method of Example 35 to generate the title product.

Sources & evidence

ORD record
ord-7afd5130b035405cac4ed517aedc31ed
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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