Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18800782, compound

HRID 849127Notes

Reaction equation

HRID 849127 reaction equation
[O:1]1[CH:5]=[CH:4][C:3]([CH2:6][CH2:7][CH:8]2[NH:14][C:13](=[O:15])[CH2:12][CH2:11][CH2:10][CH2:9]2)=[CH:2]1.F[B-](F)(F)F.[CH3:21][O+](C)C>C(Cl)Cl>[O:1]1[CH:5]=[CH:4][C:3]([CH2:6][CH2:7][CH:8]2[CH2:9][CH2:10][CH2:11][CH2:12][C:13]([O:15][CH3:21])=[N:14]2)=[CH:2]1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 18800721HCID 18800721, compound

Product 1

HCID 18800782HCID 18800782, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 170 is reacted with trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-dad00e98f8b5466f96134e48175e68a0
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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