Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18800755, compound

HRID 849129Notes

Reaction equation

HRID 849129 reaction equation
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=[CH:7][CH:8]1[NH:14][C:13](=[O:15])[CH2:12][CH2:11][CH2:10][CH2:9]1.F[B-](F)(F)F.[CH3:21][O+](C)C>C(Cl)Cl>[CH3:21][O:15][C:13]1[CH2:12][CH2:11][CH2:10][CH2:9][CH:8]([CH2:7][CH2:6][C:2]2[S:1][CH:5]=[CH:4][CH:3]=2)[N:14]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 53922947HCID 53922947, compound

Product 1

HCID 18800755HCID 18800755, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 173 is reacted with trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-17cc59cd320c480c81d22775841fb06c
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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