HCID 178479064, compound → HCID 178479065, compound

HRID 849130Notes

Reaction equation

HRID 849130 reaction equation
[ClH:1].[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[CH:7]=[CH:8][CH:9]1[NH:15][C:14](=[NH:16])[CH2:13][CH2:12][CH2:11][CH2:10]1>CCO.[Pd]>[ClH:1].[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[CH2:7][CH2:8][CH:9]1[NH:15][C:14](=[NH:16])[CH2:13][CH2:12][CH2:11][CH2:10]1

Participants

4

Reactant 1

HCID 178479064HCID 178479064, compound

Product 1

HCID 178479065HCID 178479065, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

The title material of Example 175 in EtOH is hydrogenated over 10% Pd on carbon catalyst in a standard Parr apparatus by the method of Example 35 to generate the title product.

Sources & evidence

ORD record
ord-bcf1b0462d4142b3ba65503ce95de93d
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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