Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 53655723, compound

HRID 849131Notes

Reaction equation

HRID 849131 reaction equation
[O:1]=[C:2]1[NH:8][CH:7]([CH2:9][CH:10]=[CH:11][C:12]2[O:16][C:15]([C:17]([O:19][CH3:20])=[O:18])=[CH:14][CH:13]=2)[CH2:6][CH2:5][CH2:4][CH2:3]1.F[B-](F)(F)F.[CH3:26][O+](C)C>C(Cl)Cl>[CH3:26][O:1][C:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH:7]([CH2:9][CH:10]=[CH:11][C:12]2[O:16][C:15]([C:17]([O:19][CH3:20])=[O:18])=[CH:14][CH:13]=2)[N:8]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 54273187HCID 54273187, compound

Product 1

HCID 53655723HCID 53655723, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 177 is reacted with trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-4f52f3abab7c4846a7d3d2a8200329ca
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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