HCID 178497726, compound → HCID 178497727, compound

HRID 849133Notes

Reaction equation

HRID 849133 reaction equation
[ClH:1].[NH:2]=[C:3]1[NH:9][CH:8]([CH2:10][CH:11]=[CH:12][C:13]2[O:17][C:16]([C:18]([O:20][CH3:21])=[O:19])=[CH:15][CH:14]=2)[CH2:7][CH2:6][CH2:5][CH2:4]1>CCO.[Pd]>[ClH:1].[NH:2]=[C:3]1[NH:9][CH:8]([CH2:10][CH2:11][CH2:12][C:13]2[O:17][C:16]([C:18]([O:20][CH3:21])=[O:19])=[CH:15][CH:14]=2)[CH2:7][CH2:6][CH2:5][CH2:4]1

Participants

4

Reactant 1

HCID 178497726HCID 178497726, compound

Product 1

HCID 178497727HCID 178497727, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

The title material of Example 179 in EtOH is hydrogenated over 10% Pd on carbon catalyst in a standard Parr apparatus by the method of Example 35 to generate the title product.

Sources & evidence

ORD record
ord-f3c1373a231a4d2cbcb075d25c376258
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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