HCID 178479068, compound → HCID 178479069, compound

HRID 849135Notes

Reaction equation

HRID 849135 reaction equation
[ClH:1].[S:2]1[CH:6]=[CH:5][N:4]=[C:3]1[CH:7]=[CH:8][CH:9]1[NH:15][C:14](=[NH:16])[CH2:13][CH2:12][CH2:11][CH2:10]1>CCO.[Pd]>[ClH:1].[S:2]1[CH:6]=[CH:5][N:4]=[C:3]1[CH2:7][CH2:8][CH:9]1[NH:15][C:14](=[NH:16])[CH2:13][CH2:12][CH2:11][CH2:10]1

Participants

4

Reactant 1

HCID 178479068HCID 178479068, compound

Product 1

HCID 178479069HCID 178479069, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

The title material Of Example 183 in EtOH is hydrogenated over 10% Pd on carbon catalyst in a standard Parr apparatus by the method of Example 35 to generate the title product.

Sources & evidence

ORD record
ord-45da7c25053a43e89285ee5917460ea5
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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