Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18800785, compound

HRID 849136Notes

Reaction equation

HRID 849136 reaction equation
[C:1]1([CH2:7][CH:8]2[NH:14][C:13](=[O:15])[CH:12]=[CH:11][CH2:10][CH2:9]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.F[B-](F)(F)F.[CH3:21][O+](C)C>C(Cl)Cl>[CH3:21][O:15][C:13]1[CH:12]=[CH:11][CH2:10][CH2:9][CH:8]([CH2:7][C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[N:14]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 18800636HCID 18800636, compound

Product 1

HCID 18800785HCID 18800785, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of Example 187 is reacted with one equivalent of trimethyloxonium tetrafluoroborate in CH2Cl2 by the method of Example 3 to produce the title material.

Sources & evidence

ORD record
ord-91633d582ee34c6991095479c7303a3a
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

Loading…