HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 178459641, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Isopropyl chloroformate | HCID 7917 | — |
| Reactant | HCID 178451486 | HCID 178451486 | — |
| Reactant | HCID 178473725 | HCID 178473725 | — |
| Solvent | Hexane | HCID 8058 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178459641 | HCID 178459641 | 42% |
Reaction Steps
Example 358 was prepared as a light yellow solid in 42% yield from Compound C of Example 248 by the following sequence: Compound E of Example 248, using a toluene solution of isopropyl chloroformate with chromatography using 40% hexane in EtOAc and with the free base carried on; Example 354. MS: [M+H]+ =430.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011029 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-ae5ad0235d434d5a86b57399cb157de7 |
| Source note | uspto-grants-2000_01 |