HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 53730086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 15340055 | HCID 15340055 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 53730086 | HCID 53730086 | — |
Reaction Conditions
| Temperature | 0 °C |
|---|
Reaction Steps
0.35 g of 4-(1-fluoro 2-phenyl cyclopropyl) benzoic acid (mixture (B)), obtained according to Preparation 1, and 20 cm3 of dichloromethane are mixed together under an inert gas atmosphere, the mixture is cooled down to 0° C., 0.207 g of commercial oxalyl chloride and 0.01 cm3 of dimethylformamide are added, the whole is agitated for 3 hours at 20-250° C. and brought to dryness in order to collect the acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06013837 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-ae991f2322024563910cb65ba72f80e3 |
| Source note | uspto-grants-2000_01 |