HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1-propanol → HCID 70292693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1-propanol | HCID 11807 | — |
| Reactant | HCID 19368080 | HCID 19368080 | — |
| Solvent | Ethyl ether methylene chloride | HCID 21881112 | — |
| Product | HCID 70292693 | HCID 70292693 | — |
Reaction Steps
1.2 g of N'-t-butyl-N-(4-carbomethoxybenzoyl)-N'-(3-toluoyl)hydrazine was heated in 2 ml of 2-amino-2-methyl-1-propanol at 90-100° C. for 5 hours. After cooling, the mixture was diluted with ether/methylene chloride and washed with 0.1 N HCl. The organic layer was evaporated to afford 1.0 g of the corresponding amide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06013836 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-2bed7b9ecc604236981b0a29cc0989c5 |
| Source note | uspto-grants-2000_01 |