HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N'-t-butyl-N-(2-pyridinecarbonyl)-N'-benzoylhydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N'-t-butyl-N-(2-pyridinecarbonyl)hydrazine | HCID 15767542 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N'-t-butyl-N-(2-pyridinecarbonyl)-N'-benzoylhydrazine | HCID 15767541 | — |
Reaction Steps
A solution of N'-t-butyl-N-(2-pyridinecarbonyl)-hydrazine (1.0 g, 0.00518 mol) in 20 ml of toluene at 23° C. was treated sequentially with 50% sodium hydroxide (1.3 g) and benzoyl chloride (0.728 g). The mixture was stirred overnight. The solids were removed by filtration and washed with water to afford N'-t-butyl-N-(2-pyridinecarbonyl)-N'-benzoylhydrazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06013836 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-51f2435e3b72486fba8f988f8e25bf34 |
| Source note | uspto-grants-2000_01 |