HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → N'-t-butyl-N-(2-thiophenecarbonyl)-N'-benzoylhydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N'-t-butyl-N-(2-thiophenecarbonyl)hydrazine | HCID 15452035 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N'-t-butyl-N-(2-thiophenecarbonyl)-N'-benzoylhydrazine | HCID 15452003 | — |
Reaction Steps
N'-t-butyl-N-(2-thiophenecarbonyl)hydrazine (1 g) was dissolved in 10 ml toluene and treated with 50% aqueous sodium hydroxide (1.0 g) and water (2 ml) followed by benzoylchloride (0.8 g). After stirring for 14 hours at room temperature, the solid product, N'-t-butyl-N-(2-thiophenecarbonyl)-N'-benzoylhydrazine, was removed by filtration and washed with water. m.p. >190° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06013836 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-1b97bb2cfe284e74bb23fac2d6d9fd34 |
| Source note | uspto-grants-2000_01 |