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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 849785Generated: November 1, 2026

Benzoyl chloride → HCID 15452004, compound

https://huagongshe.com/reaction/849785

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzoyl chlorideHCID 7412—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 15452036HCID 15452036—
SolventWaterHCID 962—
SolventTolueneHCID 1140—
ProductHCID 15452004HCID 15452004—

Reaction Steps

N'-t-butyl-N-(2-furoyl)hydrazine (1.0 g) was dissolved in 10 ml toluene and 2 ml water. 50% aqueous sodium hydroxide (1.0 g) was added followed by benzoylchloride (0.8 g). After stirring for 14 hours at room temperature, the solid product, N'-t-butyl-N-(2-furoyl)-N'-benzoylhydrazine, was removed by filtration and washed with water. m.p. 160-162° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06013836
Source datasetuspto-grants-2000_01
ORD IDord-da5cb1c71c83468896c51daa8679b66b
Source noteuspto-grants-2000_01