HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylphenyl isocyanate → N'-t-butyl-N'-benzoyl-N-[N-(4-tolyl)aminocarbonyl]hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylphenyl isocyanate | HCID 69325 | — |
| Reactant | N-(tert-butyl)benzohydrazide | HCID 1275961 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N'-t-butyl-N'-benzoyl-N-[N-(4-tolyl)aminocarbonyl]hydrazine | HCID 15452014 | 36.9% |
Reaction Steps
N't-butyl-N'-benzoylhydrazine (0.8 g) and p-methylphenylisocyanate (0.9 g) were stirred in diethylether (10 ml) at 23° C. for 15 hours. The reaction mixture was diluted with ether and filtered to afford 0.5 g of solid product: m.p. 208-210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06013836 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-889f68f7d3d6457bb4ad652bd509b084 |
| Source note | uspto-grants-2000_01 |