N'-t-butyl-N'-(3-methylbenzoyl)hydrazine → N'-t-butyl-N-(2-phenyl-3-methylpentanoyl)-N'-(3-toluoyl)hydrazine

Participants

Role	Name	HCID	Charge
Reactant	N'-t-butyl-N'-(3-methylbenzoyl)hydrazine	HCID 15452040	—
Reactant	3-Methyl-2-phenylvaleryl chloride	HCID 21886026	—
Catalyst	Sodium Hydroxide	HCID 14798	—
Solvent	Toluene	HCID 1140	—
Product	N'-t-butyl-N-(2-phenyl-3-methylpentanoyl)-N'-(3-toluoyl)hydrazine	HCID 15452019	—

Reaction Steps

To a stirred suspension of N'-t-butyl-N'-(3-toluoyl)hydrazine (0.7 g) in toluene (10 ml) and aqueous sodium hydroxide (12 drops of 50% aqueous sodium hydroxide) was added dropwise 2-phenyl-3-methyl-pentanoyl chloride (1.0 g). The reaction mixture was stirred overnight, diluted with hexanes and the solids filtered. The solids were washed with hexane and air dried.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06013836
Source dataset	uspto-grants-2000_01
ORD ID	ord-bcdc5b0e92e1419cba25cc680b139b5c
Source note	uspto-grants-2000_01