Phenol → HCID 226704, compound

HRID 849895Notes

Reaction equation

HRID 849895 reaction equation
[CH2:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[OH:9])[CH3:2].Cl[C:11]([CH3:19])([CH2:13][CH2:14][C:15](Cl)([CH3:17])[CH3:16])[CH3:12].C1(O)C=CC=CC=1>>[CH2:1]([C:3]1[C:4]([OH:9])=[CH:5][C:6]2[C:11]([CH3:19])([CH3:12])[CH2:13][CH2:14][C:15]([CH3:17])([CH3:16])[C:7]=2[CH:8]=1)[CH3:2]

Participants

4

Reactant 3

HCID 996PhenolHCID 69972-EthylphenolHCID 80360Hexane, 2,5-dichloro-2,5-dimethyl-

Product 1

HCID 226704HCID 226704, compound

Procedure

In a manner similar to Example 7(a) above, by the reaction of 15 g (0.123 mol) of 2-ethylphenol with 22.5 g (0.123 mol) of 2,5-dichloro-2,5-dimethylhexane, 25.4 g (89%) of the expected phenol of melting point 88-9° C. were obtained after chromatography on a silica column eluted with dichloromethane.

Workup

  1. customwere obtained after chromatography on a silica column
  2. washeluted with dichloromethane

Sources & evidence

ORD record
ord-2fb0038836334f2faf2792371ed5342c
Source dataset
uspto-grants-2000_01
Patent number
US06015569

Reaction notes

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