HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzaldehyde → HCID 9839602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Reactant | 5,5,8,8-Tetramethyl-5,6,7,8-tetrahydronaphthalen-2-ol | HCID 268786 | — |
| Product | HCID 9839602 | HCID 9839602 | — |
Reaction Steps
In a manner similar to Example 1(a) above, by the reaction of 5.3 g (15 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthol with 3.1 g (16.5 mmol) of 4-bromobenzaldehyde, 2.4 g of the expected aldehyde of melting point 75-6° C. were obtained after purification by chromatography on a silica column eluted with a mixture of dichloromethane and hexane (50/50).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06015569 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-d3f9cf21cc7043399382b408ed9ac5fb |
| Source note | uspto-grants-2000_01 |