Nicotinic Acid → HCID 23700586, compound

HRID 849983Notes

Reaction equation

HRID 849983 reaction equation
[C:1]([OH:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[N:4][CH:3]=1.C(=O)([O-])[O-].[Cs+:14].[Cs+]>CO>[C:1]([O-:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[N:4][CH:3]=1.[Cs+:14]

Participants

4

Reactant 2

HCID 938Nicotinic AcidHCID 10796Cesium carbonate

Product 1

HCID 23700586HCID 23700586, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Nicotinic acid (0.86 g, 7 mmol) and cesium carbonate (1.14 g, 3.5 mmol) were swirled in methanol (60 ml) until a clear solution resulted. Methanol was removed in vacuo to yield cesium nicotinate as a white solid.

Workup

  1. customresulted
  2. customMethanol was removed in vacuo

Sources & evidence

ORD record
ord-5ddb1dba266e4c4691ad21620da0bf36
Source dataset
uspto-grants-2000_01
Patent number
US06015821

Reaction notes

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