HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 18354611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(Bromomethyl)-4-(trifluoromethyl)benzene | HCID 123062 | — |
| Reactant | 3-Hydroxybenzamide | HCID 342403 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 18354611 | HCID 18354611 | — |
Reaction Steps
3-hydroxybenzamide (0.137 g; 1 mmol) was dissolved in anhydrous acetonitrile (20 ml) under a nitrogen atmosphere. To this was added potassium carbonate (0.138 g; 1 mmol) and 4-(trifluoromethyl)benzyl bromide (0.155 ml; 1 mmol). This mixture was left to reflux for 17 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06015827 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-191d47be0afd4556a3fc5cc702dff9fa |
| Source note | uspto-grants-2000_01 |