1-(Chloromethoxy)-2-methoxyethane → HCID 19365953, compound

HRID 850112Notes

Reaction equation

HRID 850112 reaction equation
[NH:1]1[CH:5]=[CH:4][N:3]=[N:2]1.[CH3:6][O:7][CH2:8][CH2:9][O:10][CH2:11]Cl>>[CH3:6][O:7][CH2:8][CH2:9][O:10][CH2:11][N:1]1[CH:5]=[CH:4][N:3]=[N:2]1

Participants

3

Reactant 2

HCID 775901-(Chloromethoxy)-2-methoxyethaneHCID 178418936HCID 178418936, compound

Product 1

HCID 19365953HCID 19365953, compound

Procedure

The title compound was prepared from 1,2,3-triazole and 2-methoxyethoxymethyl chloride, by a similar method to that of Preparation 40, as a colourless oil which was characterised by 1H-NMR spectroscopy (300 MHz, CDCl3): δ=3.31(s,3H), 3.46(m,2H), 3.62(m,2H), 5.77(s,2H), 7.73(s,1H),7.75(s,1H) ppm.

Workup

  1. customof Preparation 40

Sources & evidence

ORD record
ord-d83ede1457b64e49a4d28d4e40877ba1
Source dataset
uspto-grants-2000_01
Patent number
US06015825

Reaction notes

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